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Synthesis of hydroxyapatite nano-powders from agurong (jagora asperata) shells sol-gel method [manuscript] / Anthony Clarence C. Banan, Freidrich A. Cusipag, Mark Daryll B. Diaz, Carlos Miguel M. Tagacay, Kliff Yran S. Villanueva.

by Banan, Anthony Clarence C., author.
Physical details: x, 64 pages ; 28 cm. Year: 2024
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Academic Research Academic Research Academic Research Section Academic Research C'ENG 0042 2024 c.1 (Browse shelf) Available CHEMICAL0042
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Thesis (B.S.) -- Cagayan State University, 2024.
Includes bibliographical references.

Nanotechnology significantly advances various fields by manipulating materials at the nanoscale, particularly nanoparticles like hydroxyapatite (HAp) nano- powder. Known for its excellent biocompatibility and osteoconductivity, HAp finds extensive use in biomedical, cosmetic, catalytic, and energy storage applications. This study investigates the synthesis of hydroxyapatite nano-powders from Agurong (Jagora asperata) shells using Sol-Gel Method. The synthesized HAp nano-powders were characterized using X-Ray Diffraction (XRD) analysis, nano-powder size calculation using Scherrer equation, and Scanning Electron Microscopy - Energy Dispersive Spectroscopy (SEM-EDS) analysis. The XRD analysis showed a similar chemical structure to commercial HAp. The Scherrer equation indicated a particle size of 68.65 nanometers, which is within the expected range of less than 100 nanometers, meeting the criteria for nano-scale crystallites. SEM-EDS analysis confirmed the identity of Agurong HAP with a Ca/P ratio of 1.79, which is within the acceptable range of the Ca/P ratio of a standard hydroxyapatite of 1.4 to 2.0. Through the Sol-Gel method, 25.71 grams of HAP nano-powders were successfully synthesized from 500 grams of raw Agurong, demonstrating the potential of this underutilized resource from the Philippines for the production of HAP nano-powders.

Keywords: Agurong, Hydroxyapatite, Nano-powders, Nanotechnology, Sol-Gel Method.

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